anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

Base Information

Chemical Name:anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide
CAS No.:97522-72-0
Molecular Formula:C₁₅H₁₂N₂O₂S
Molecular Weight:284.338
Hs Code.:

Synonyms:anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

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Chemical Property of anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

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Technology Process of anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

There total 4 articles about anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 108-24-7
acetic anhydride

: 97522-70-8
anhydro-2-(3-aminophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

: 97522-72-0
anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

Guidance literature:: Heating;
DOI:10.1021/jm00149a023

Reference yield:

: 2127-03-9
2,2'-dipyridyldisulphide

: 97522-72-0
anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / tri-n-butylphosphine / tetrahydrofuran

2: 65 percent / H₂ / 10percent Pd/C / 2-methoxy-ethanol / 760 Torr

3: 78 percent / Heating

With tributylphosphine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 2-methoxy-ethanol;
DOI:10.1021/jm00149a023

Reference yield:

: 42164-79-4
3-nitromandelic acid

: 97522-72-0
anhydro-2-(3-acetamidophenyl)-3-hydroxythiazolo<3,2-a>pyridinium hydroxide

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / tri-n-butylphosphine / tetrahydrofuran

2: 65 percent / H₂ / 10percent Pd/C / 2-methoxy-ethanol / 760 Torr

3: 78 percent / Heating

With tributylphosphine; hydrogen; palladium on activated charcoal; In tetrahydrofuran; 2-methoxy-ethanol;
DOI:10.1021/jm00149a023