C₃₀H₄₂O₇

Base Information

• Chemical Name: C₃₀H₄₂O₇
• CAS No.: 1309956-00-0
• Molecular Formula: C₃₀H₄₂O₇
• Molecular Weight: 514.659

Synonyms:C₃₀H₄₂O₇

Chemical Property of C₃₀H₄₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₄₂O₇

There total 25 articles about C₃₀H₄₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C27H42O3Si (1309955-89-2) → C30H42O7 (1309956-00-0)

Guidance literature:

Multi-step reaction with 22 steps

1.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 25 - 60 °C / Inert atmosphere

2.2: 15 h / 25 °C / Inert atmosphere

3.1: borane-THF / tetrahydrofuran / 72 h / 0 °C / Inert atmosphere

3.2: 0 - 25 °C / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Microwave irradiation; Inert atmosphere

6.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

7.1: sodium hydride / methanol / 0 - 25 °C / Inert atmosphere

8.1: triethylamine / dichloromethane / 4 h / 25 °C / Inert atmosphere

9.1: potassium tert-butylate / tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

10.1: ammonia; lithium / tetrahydrofuran; ethanol / -78 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

11.2: 0.5 h / 0 °C / Inert atmosphere

12.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 3 h / -78 °C / Inert atmosphere

13.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 60 °C / Inert atmosphere

13.2: 15 h / 20 °C / Inert atmosphere

14.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Inert atmosphere; Microwave irradiation

15.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

16.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

17.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

17.2: 1 h / -78 °C / Inert atmosphere

18.1: formic acid; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 75 °C / Inert atmosphere

19.1: borane-THF / tetrahydrofuran / 15 h / Inert atmosphere; Reflux

19.2: 0 - 20 °C / Inert atmosphere

19.3: 0 - 20 °C / Inert atmosphere

20.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

21.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium tert-butoxide / tetrahydrofuran / 1 h / 70 °C / Inert atmosphere

22.1: tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium tetrahydroborate; formic acid; borane-THF; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; palladium diacetate; sodium hexamethyldisilazane; lithium; sodium hydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium tert-butoxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Hydroboration reaction / 8.1: Michael addition / 9.1: Robinson cyclization / 19.1: Hydroboration reaction;

DOI:10.1021/ol200966z

Reference yield:

C34H50O3Si (1309956-03-3) → C30H42O7 (1309956-00-0)

Guidance literature:

Multi-step reaction with 20 steps

1.1: borane-THF / tetrahydrofuran / 72 h / 0 °C / Inert atmosphere

1.2: 0 - 25 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Microwave irradiation; Inert atmosphere

4.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

5.1: sodium hydride / methanol / 0 - 25 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 4 h / 25 °C / Inert atmosphere

7.1: potassium tert-butylate / tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

8.1: ammonia; lithium / tetrahydrofuran; ethanol / -78 °C / Inert atmosphere

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

9.2: 0.5 h / 0 °C / Inert atmosphere

10.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 3 h / -78 °C / Inert atmosphere

11.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 60 °C / Inert atmosphere

11.2: 15 h / 20 °C / Inert atmosphere

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Inert atmosphere; Microwave irradiation

13.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

14.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

15.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

15.2: 1 h / -78 °C / Inert atmosphere

16.1: formic acid; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 75 °C / Inert atmosphere

17.1: borane-THF / tetrahydrofuran / 15 h / Inert atmosphere; Reflux

17.2: 0 - 20 °C / Inert atmosphere

17.3: 0 - 20 °C / Inert atmosphere

18.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

19.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium tert-butoxide / tetrahydrofuran / 1 h / 70 °C / Inert atmosphere

20.1: tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium tetrahydroborate; formic acid; borane-THF; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; palladium diacetate; sodium hexamethyldisilazane; lithium; sodium hydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium tert-butoxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; 1.1: Hydroboration reaction / 6.1: Michael addition / 7.1: Robinson cyclization / 17.1: Hydroboration reaction;

DOI:10.1021/ol200966z

Reference yield:

C27H44O3Si (1309956-02-2) → C30H42O7 (1309956-00-0)

Guidance literature:

Multi-step reaction with 21 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 25 - 60 °C / Inert atmosphere

1.2: 15 h / 25 °C / Inert atmosphere

2.1: borane-THF / tetrahydrofuran / 72 h / 0 °C / Inert atmosphere

2.2: 0 - 25 °C / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 15 h / 20 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Microwave irradiation; Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: sodium hydride / methanol / 0 - 25 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 4 h / 25 °C / Inert atmosphere

8.1: potassium tert-butylate / tert-butyl alcohol / 0.5 h / 25 °C / Inert atmosphere

9.1: ammonia; lithium / tetrahydrofuran; ethanol / -78 °C / Inert atmosphere

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C / Inert atmosphere

10.2: 0.5 h / 0 °C / Inert atmosphere

11.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 3 h / -78 °C / Inert atmosphere

12.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 60 °C / Inert atmosphere

12.2: 15 h / 20 °C / Inert atmosphere

13.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 130 °C / Inert atmosphere; Microwave irradiation

14.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere

15.1: Dess-Martin periodane / dichloromethane / 2 h / 0 °C / Inert atmosphere

16.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere

16.2: 1 h / -78 °C / Inert atmosphere

17.1: formic acid; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 75 °C / Inert atmosphere

18.1: borane-THF / tetrahydrofuran / 15 h / Inert atmosphere; Reflux

18.2: 0 - 20 °C / Inert atmosphere

18.3: 0 - 20 °C / Inert atmosphere

19.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

20.1: 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; lithium tert-butoxide / tetrahydrofuran / 1 h / 70 °C / Inert atmosphere

21.1: tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium tetrahydroborate; formic acid; borane-THF; potassium tert-butylate; tetrabutyl ammonium fluoride; ammonia; palladium diacetate; sodium hexamethyldisilazane; lithium; sodium hydride; Dess-Martin periodane; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium tert-butoxide; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; 2.1: Hydroboration reaction / 7.1: Michael addition / 8.1: Robinson cyclization / 18.1: Hydroboration reaction;

DOI:10.1021/ol200966z

upstream raw materials:

C₂₇H₄₂O₃Si

C₂₇H₄₄O₃Si

C₃₄H₅₀O₃Si

C₃₄H₅₂O₄Si

Downstream raw materials:

C₃₁H₄₄O₇

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