<<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester

Base Information

Chemical Name:<<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester
CAS No.:97219-42-6
Molecular Formula:C₁₉H₂₂ClN₃O₄
Molecular Weight:391.854
Hs Code.:

Synonyms:<<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester

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Chemical Property of <<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester

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Technology Process of <<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester

There total 6 articles about <<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 4530-20-5
BOC-glycine

: 97219-41-5
(2-chlorophenyl)<1-(methylamino)-1H-pyrrol-2-yl>methanone

: 97219-42-6
<<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; for 5h; Ambient temperature;

Reference yield:

: 609-65-4
o-chlorobenzoyl chloride

: 97219-42-6
<<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 45 percent / ZnCl₂ / 1,2-dichloro-ethane / 4 h / 60 °C

2: 94 percent / 40percent aq. methylamine / aq. ethanol / 2 h

3: 77 percent / NaHCO₃ / CH₂Cl₂ / 2.5 h / Heating

4: 57 percent / dimethylformamide / 8 h / Ambient temperature

5: 85 percent / NaOH / ethanol; H₂O / 18 h / Heating

6: 68 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 5 h / Ambient temperature

With sodium hydroxide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; methylamine; zinc(II) chloride; In ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 97219-75-5
(1-amino-1H-pyrrol-2-yl)(2-chlorophenyl)methanone

: 97219-42-6
<<<2-<2-chlorobenzoyl>-1H-pyrrol-1-yl>methylamino>carbonyl>methylcarbamic acid 2-methylpropyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / NaHCO₃ / CH₂Cl₂ / 2.5 h / Heating

2: 57 percent / dimethylformamide / 8 h / Ambient temperature

3: 85 percent / NaOH / ethanol; H₂O / 18 h / Heating

4: 68 percent / dicyclohexylcarbodiimide / CH₂Cl₂ / 5 h / Ambient temperature

With sodium hydroxide; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;