2-(5-bromo-2-{[(4-methylphenyl)sulfonyl]oxy}phenyl)-2-oxo-1-phenylethyl acetate

Base Information

Chemical Name:2-(5-bromo-2-{[(4-methylphenyl)sulfonyl]oxy}phenyl)-2-oxo-1-phenylethyl acetate
CAS No.:1187442-45-0
Molecular Formula:C₂₃H₁₉BrO₆S
Molecular Weight:503.37
Hs Code.:

Synonyms:2-(5-bromo-2-{[(4-methylphenyl)sulfonyl]oxy}phenyl)-2-oxo-1-phenylethyl acetate

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Chemical Property of 2-(5-bromo-2-{[(4-methylphenyl)sulfonyl]oxy}phenyl)-2-oxo-1-phenylethyl acetate

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Technology Process of 2-(5-bromo-2-{[(4-methylphenyl)sulfonyl]oxy}phenyl)-2-oxo-1-phenylethyl acetate

There total 1 articles about 2-(5-bromo-2-{[(4-methylphenyl)sulfonyl]oxy}phenyl)-2-oxo-1-phenylethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 6286-84-6
2,4-dibromophenyl 4-methylbenzenesulfonate

: 1638-63-7
2-acetoxy-2-phenylacetyl chloride

: 1187442-45-0
2-(5-bromo-2-{[(4-methylphenyl)sulfonyl]oxy}phenyl)-2-oxo-1-phenylethyl acetate

Guidance literature:: 2,4-dibromophenyl 4-methylbenzenesulfonate; With lithium chloride; zinc; In tetrahydrofuran; at 50 ℃; for 14h; Inert atmosphere;

With CCl₂CuN^(2-)*2Li⁽¹⁺⁾; In tetrahydrofuran; at -20 ℃; for 0.25h; Inert atmosphere;

2-acetoxy-2-phenylacetyl chloride; In tetrahydrofuran; at -20 - 25 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1002/chem.200900575