Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>

Base Information

Chemical Name:Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>
CAS No.:75999-18-7
Molecular Formula:C₁₅H₁₇N₃O₃
Molecular Weight:287.318
Hs Code.:

Synonyms:Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>

Suppliers and Price of Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>

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Technology Process of Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>

There total 3 articles about Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 75999-07-4
5-(4-Hydroxybenzyl)-2,4-dimethylpyrimidin-6-ol

: 624-83-9
methyl isocyanate

: 75999-18-7
Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 168h; Ambient temperature;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 75999-18-7
Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>

Guidance literature:: Multi-step reaction with 3 steps

1: 1) piperidine, 2) H₂ / 2) Raney-Ni / 1) benzene, reflux, 7 h, 2) ethanol, room temperature, 1.5 d

2: 68 percent / NaOEt / ethanol / 96 h / Ambient temperature

3: 86 percent / Et₃N / dimethylformamide / 168 h / Ambient temperature

With piperidine; hydrogen; sodium ethanolate; triethylamine; nickel; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 52252-58-1
2-(4-Hydroxybenzyl)acetessigsaeure-ethylester

: 75999-18-7
Methylcarbaminsaeure-<4-(6-hydroxy-2,4-dimethylpyrimidin-5-ylmethyl)phenylester>

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / NaOEt / ethanol / 96 h / Ambient temperature

2: 86 percent / Et₃N / dimethylformamide / 168 h / Ambient temperature

With sodium ethanolate; triethylamine; In ethanol; N,N-dimethyl-formamide;