(3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal

Base Information

Chemical Name:(3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal
CAS No.:1351977-06-4
Molecular Formula:C₂₉H₅₄O₅Si₂
Molecular Weight:538.916
Hs Code.:

Synonyms:(3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal

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Chemical Property of (3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal

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Technology Process of (3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal

There total 14 articles about (3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₉H₅₆O₅Si₂

: 1351977-06-4
(3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal

: C₂₉H₅₄O₅Si₂

Guidance literature:: With pyridine; Dess-Martin periodane; In dichloromethane; at 23 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol203130b

Reference yield:

: C₃₁H₅₈O₆Si₂

: 1351977-06-4
(3S,5S)-5-(tert-butyldimethylsilyloxy)-7-(4-methoxybenzyloxy)-4,4-dimethyl-3-(triethylsilyloxy)heptanal

: C₂₉H₅₄O₅Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride / hexane; dichloromethane / 3 h / -78 °C / Inert atmosphere

2: pyridine; Dess-Martin periodane / dichloromethane / 2 h / 23 °C / Inert atmosphere

With pyridine; diisobutylaluminium hydride; Dess-Martin periodane; In hexane; dichloromethane;
DOI:10.1021/ol203130b