5,6-dihydro-3-methyl-2-phenylbenzoquinoline

Base Information

Chemical Name:5,6-dihydro-3-methyl-2-phenylbenzoquinoline
CAS No.:130445-97-5
Molecular Formula:C₂₀H₁₇N
Molecular Weight:271.362
Hs Code.:

5,6-dihydro-3-methyl-2-phenylbenzo<h>quinoline

Synonyms:5,6-dihydro-3-methyl-2-phenylbenzoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5,6-dihydro-3-methyl-2-phenylbenzoquinoline

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Technology Process of 5,6-dihydro-3-methyl-2-phenylbenzoquinoline

There total 3 articles about 5,6-dihydro-3-methyl-2-phenylbenzoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 130445-69-1
3-cyano-5,6-dihydro-4-(methylthio)-2-phenylbenzoquinoline

: 130445-97-5
5,6-dihydro-3-methyl-2-phenylbenzoquinoline

Guidance literature:: W-4 Raney nickel; In ethanol; for 3h; Heating;
DOI:10.1016/S0040-4020(01)81540-4

Reference yield:

: 57663-21-5
2-bis(methylthio)methylene-1-tetralone

: 130445-97-5
5,6-dihydro-3-methyl-2-phenylbenzoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1) nBuLi / 1) THF, -78 deg C, 0.5h, 2) r.t., 20h

2: 71 percent / W-4 Raney Nickel / ethanol / 3 h / Heating

With n-butyllithium; W-4 Raney nickel; In ethanol;
DOI:10.1016/S0040-4020(01)81540-4

Reference yield:

: 100-47-0
benzonitrile

: 130445-97-5
5,6-dihydro-3-methyl-2-phenylbenzoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 1) nBuLi / 1) THF, -78 deg C, 0.5h, 2) r.t., 20h

2: 71 percent / W-4 Raney Nickel / ethanol / 3 h / Heating

With n-butyllithium; W-4 Raney nickel; In ethanol;
DOI:10.1016/S0040-4020(01)81540-4