3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide

Base Information

Chemical Name:3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide
CAS No.:947530-56-5
Molecular Formula:C₂₇H₂₆BrNO₄
Molecular Weight:508.412
Hs Code.:

Synonyms:3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide

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Technology Process of 3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide

There total 1 articles about 3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 866756-37-8
N-[2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-N-(4-methoxybenzyl)amine

: 7299-58-3
phenylpropiolyl chloride

: 947530-56-5
3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 40h;
DOI:10.1021/ol071079g

Reference yield: 81.0%

: 947530-56-5
3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide

: 947530-73-6
1-benzylidene-7,8-dimethoxy-3-(4-methoxybenzyl)-1,3,4,5-tetrahydrobenzo[d]azepin-2-one

Guidance literature:: With sodium formate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 110 ℃; for 0.25h; microwave irradiation;
DOI:10.1021/ol071079g

Reference yield: 18.0%

: 947530-56-5
3-phenylpropynoic acid [2-(2-bromo-4,5-dimethoxyphenyl)ethyl]-(4-methoxybenzyl)amide

: potassium vinyltrifluoroborate

: (Z)-7,8-dimethoxy-3-(4-methoxybenzyl)-1-(1-phenylallylidene)-4,5-dihydro-1H-benz[d]azepin-2(3H)-one

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium phosphate; In water; N,N-dimethyl-formamide; at 115 ℃; for 0.583333h; Microwave irradiation; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.joc.5b00670