Technology Process of C29H30N6O4
There total 5 articles about C29H30N6O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-pyrrolidinon;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 5 ℃;
for 1h;
Inert atmosphere;
C26H27N5O6S;
In
N,N-dimethyl-formamide; mineral oil;
at 5 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere
2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
3.1: triethylamine / dichloromethane / 1 h / 5 - 20 °C / Inert atmosphere
4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere
4.2: 5 - 20 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; sodium hydride; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium acetate; palladium diacetate / 1,4-dioxane / 18 h / 100 °C / Inert atmosphere
2.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 18 h / 80 °C / Inert atmosphere
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
4.1: triethylamine / dichloromethane / 1 h / 5 - 20 °C / Inert atmosphere
5.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere
5.2: 5 - 20 °C
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tetrabutyl ammonium fluoride; potassium acetate; palladium diacetate; sodium hydride; triethylamine;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;