Technology Process of C15H18O
There total 4 articles about C15H18O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C15H20O;
With
oxalyl dichloride; dimethyl sulfoxide;
In
dichloromethane;
at -78 ℃;
for 0.333333h;
Inert atmosphere;
With
triethylamine;
In
dichloromethane;
at 20 ℃;
for 0.333333h;
Inert atmosphere;
DOI:10.1002/anie.201400080
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: lithium chloride / dimethyl sulfoxide; water / 160 °C
2.1: n-butyllithium / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C / Inert atmosphere
4.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere
4.2: 0.33 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; dimethyl sulfoxide; lithium chloride;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/anie.201400080
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 0 °C / Inert atmosphere
2.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.33 h / -78 °C / Inert atmosphere
2.2: 0.33 h / 20 °C / Inert atmosphere
With
lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide;
In
diethyl ether; dichloromethane;
DOI:10.1002/anie.201400080
