ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate

Base Information

Chemical Name:ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate
CAS No.:1380312-59-3
Molecular Formula:C₁₃H₁₅BrN₆O₂
Molecular Weight:367.205
Hs Code.:

Synonyms:ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate

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Chemical Property of ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate

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Technology Process of ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate

There total 2 articles about ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1380312-58-2
ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)ethylidene]hydrazinecarboxylate

: 1380312-59-3
ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate

Guidance literature:: With bromine; In 1,4-dioxane; diethyl ether; at 20 ℃; for 24h;
DOI:10.1002/ejoc.201101826

Reference yield:

: 120869-86-5
5-acetyl-1-benzyl-1H-tetrazole

: 1380312-59-3
ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 1 h / 120 °C / Inert atmosphere

2: bromine / 1,4-dioxane; diethyl ether / 24 h / 20 °C

With bromine; toluene-4-sulfonic acid; In 1,4-dioxane; diethyl ether; toluene;
DOI:10.1002/ejoc.201101826