1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate

Base Information

Chemical Name:1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate
CAS No.:1380312-62-8
Molecular Formula:C₁₈H₂₂N₆O₄
Molecular Weight:386.41
Hs Code.:

Synonyms:1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate

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Chemical Property of 1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate

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Technology Process of 1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate

There total 3 articles about 1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1380312-59-3
ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)-2-bromoethylidene]hydrazinecarboxylate

: 80-62-6,114512-63-9,143476-91-9,25188-98-1,9011-14-7
methacrylic acid methyl ester

: 1380312-62-8
1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate

Guidance literature:: With sodium carbonate; In dichloromethane; at 20 ℃; for 23h;
DOI:10.1002/ejoc.201101826

Reference yield:

: 120869-86-5
5-acetyl-1-benzyl-1H-tetrazole

: 1380312-62-8
1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 1 h / 120 °C / Inert atmosphere

2: bromine / 1,4-dioxane; diethyl ether / 24 h / 20 °C

3: sodium carbonate / dichloromethane / 23 h / 20 °C

With bromine; sodium carbonate; toluene-4-sulfonic acid; In 1,4-dioxane; diethyl ether; dichloromethane; toluene;
DOI:10.1002/ejoc.201101826

Reference yield:

: 1380312-58-2
ethyl 2-[1-(1-benzyl-1H-tetrazol-5-yl)ethylidene]hydrazinecarboxylate

: 1380312-62-8
1-ethyl 6-methyl 3-(1-benzyl-1H-tetrazol-5-yl)-6-methyl-1,4,5,6-tetrahydropyridazine-1,6-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / 1,4-dioxane; diethyl ether / 24 h / 20 °C

2: sodium carbonate / dichloromethane / 23 h / 20 °C

With bromine; sodium carbonate; In 1,4-dioxane; diethyl ether; dichloromethane;
DOI:10.1002/ejoc.201101826