methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate

Base Information

Chemical Name:methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate
CAS No.:936716-41-5
Molecular Formula:C₁₅H₁₆F₃N₃OS
Molecular Weight:343.373
Hs Code.:

Synonyms:methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate

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Chemical Property of methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate

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Technology Process of methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate

There total 4 articles about methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 824390-04-7
4-(2-(trifluoromethyl)phenoxy)piperidine

: 10191-60-3
dimethyl N-cyanodithioiminocarbonate

: 936716-41-5
methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate

Guidance literature:: In ethanol; Heating;
DOI:10.1016/j.bmcl.2011.08.037

Reference yield:

: 921605-76-7
tert-butyl 4-[2-(trifluoromethyl)phenoxy]-piperidine-1-carboxylate

: 936716-41-5
methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 10 h / 0 - 20 °C

2: ethanol / 0.5 h / Heating / reflux

With trifluoroacetic acid; In ethanol; dichloromethane;

Reference yield:

: 444-30-4
2-(trifluoromethyl)phenol

: 936716-41-5
methyl N-cyano-[2-(trifluoromethyl)phenoxy]piperidine-1-carbimidothioate

Guidance literature:: Multi-step reaction with 3 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 16 h / 0 - 20 °C

2: trifluoroacetic acid / dichloromethane / 10 h / 0 - 20 °C

3: ethanol / 0.5 h / Heating / reflux

With triphenylphosphine; trifluoroacetic acid; diethylazodicarboxylate; In tetrahydrofuran; ethanol; dichloromethane;