Technology Process of C42H44ClNO20
There total 6 articles about C42H44ClNO20 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanol; sodium methylate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 0 ℃;
DOI:10.1021/jm970589l
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 55 percent / silver oxide / acetonitrile / 4 h / Ambient temperature
2: 90 percent / NaBH4, silica gel HL60 / CHCl3; propan-2-ol / 0.75 h / 0 °C
3: 66 percent / Et3N / CH2Cl2; acetonitrile / 1.5 h / 0 °C
4: 75 percent / Et3N / dimethylformamide / 2 h / Ambient temperature
5: 55 percent / NaOMe, MeOH / dimethylformamide; tetrahydrofuran / 0 °C
With
methanol; sodium tetrahydroborate; sodium methylate; silica gel; triethylamine; silver(l) oxide;
In
tetrahydrofuran; dichloromethane; chloroform; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;
DOI:10.1021/jm970589l
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / NaBH4, silica gel HL60 / CHCl3; propan-2-ol / 0.75 h / 0 °C
2: 66 percent / Et3N / CH2Cl2; acetonitrile / 1.5 h / 0 °C
3: 75 percent / Et3N / dimethylformamide / 2 h / Ambient temperature
4: 55 percent / NaOMe, MeOH / dimethylformamide; tetrahydrofuran / 0 °C
With
methanol; sodium tetrahydroborate; sodium methylate; silica gel; triethylamine;
In
tetrahydrofuran; dichloromethane; chloroform; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;
DOI:10.1021/jm970589l
