Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester

Base Information

Chemical Name:Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester
CAS No.:110451-82-6
Molecular Formula:C₁₉H₂₂O₄
Molecular Weight:314.381
Hs Code.:

Synonyms:Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester

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Chemical Property of Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester

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Technology Process of Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester

There total 9 articles about Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110451-72-4
Acetic acid 4-benzyloxy-3-(2-methoxymethoxy-phenyl)-butyl ester

: 110451-82-6
Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester

Guidance literature:: With sulfuric acid; acetic acid; In water; at 60 ℃; for 24h;

Reference yield:

: 80885-30-9,81028-03-7,69152-88-1
(E)-4-(benzyloxy)-2-buten-1-ol

: 110451-82-6
Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: phosphorus tribromide / diethyl ether / 0 degC, 2 h then allowed to warm to room temperature

2: potassium carbonate / acetone / 16 h / Heating

3: 72 percent / neat (no solvent) / 0.5 h / Heating

4: 92 percent / sodium hydride / dimethylformamide / Ambient temperature

5: 76 percent / 9-borabicyclo<3,3,1>nonane, aq. sodium hydroxide, hydrogen peroxide / ethanol

6: pyridine / 16 h / 20 °C

7: acetic acid, sulphuric acid / H₂O / 24 h / 60 °C

With pyridine; sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; dihydrogen peroxide; phosphorus tribromide; sodium hydride; potassium carbonate; acetic acid; In diethyl ether; ethanol; water; N,N-dimethyl-formamide; acetone;

Reference yield:

: 91142-50-6
4-benzyloxy-2-butyn-1-ol

: 110451-82-6
Acetic acid 4-benzyloxy-3-(2-hydroxy-phenyl)-butyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 65 percent / lithium aluminium hydride / tetrahydrofuran

2: phosphorus tribromide / diethyl ether / 0 degC, 2 h then allowed to warm to room temperature

3: potassium carbonate / acetone / 16 h / Heating

4: 72 percent / neat (no solvent) / 0.5 h / Heating

5: 92 percent / sodium hydride / dimethylformamide / Ambient temperature

6: 76 percent / 9-borabicyclo<3,3,1>nonane, aq. sodium hydroxide, hydrogen peroxide / ethanol

7: pyridine / 16 h / 20 °C

8: acetic acid, sulphuric acid / H₂O / 24 h / 60 °C

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; 9-borabicyclo[3.3.1]nonane dimer; sulfuric acid; dihydrogen peroxide; phosphorus tribromide; sodium hydride; potassium carbonate; acetic acid; In tetrahydrofuran; diethyl ether; ethanol; water; N,N-dimethyl-formamide; acetone;