C₄₄H₇₈N₄O₃

Base Information

Chemical Name:C₄₄H₇₈N₄O₃
CAS No.:241161-83-1
Molecular Formula:C₄₄H₇₈N₄O₃
Molecular Weight:711.128
Hs Code.:

C<sub>44</sub>H<sub>78</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:C₄₄H₇₈N₄O₃

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Chemical Property of C₄₄H₇₈N₄O₃

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Technology Process of C₄₄H₇₈N₄O₃

There total 10 articles about C₄₄H₇₈N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: C₄₄H₆₆N₄O₃

: 241161-83-1
C₄₄H₇₈N₄O₃

Guidance literature:: C₄₄H₆₆N₄O₃; With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; for 24h;

With sodium hydroxide; In tetrahydrofuran; water; at 0 ℃; Cooling with ice;

Reference yield:

: C₅₅H₇₁N₃O₄

: 241161-83-1
C₄₄H₇₈N₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1: methanol / toluene-4-sulfonic acid / dichloromethane / 3 h / 20 °C

2: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

3: 80 °C / Inert atmosphere

4: aluminum (III) chloride; lithium aluminium tetrahydride / tetrahydrofuran

With methanol; aluminum (III) chloride; lithium aluminium tetrahydride; triethylamine; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;

Reference yield:

: 3758-71-2
3α,7α,12α-trihydroxycholan-24-ol

: 241161-83-1
C₄₄H₇₈N₄O₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: dmap; triethylamine / N,N-dimethyl-formamide / 30 h / 50 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Reflux; Inert atmosphere

2.2: 110 h / Reflux

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 20 °C / Inert atmosphere; Cooling with ice

3.2: 1 h / Reflux

4.1: triethylamine / dichloromethane / 0.5 h / Inert atmosphere; Cooling with ice

5.1: dimethyl sulfoxide / 80 °C / Inert atmosphere

6.1: methanol / toluene-4-sulfonic acid / dichloromethane / 3 h / 20 °C

7.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

8.1: 80 °C / Inert atmosphere

9.1: aluminum (III) chloride; lithium aluminium tetrahydride / tetrahydrofuran

With methanol; dmap; aluminum (III) chloride; lithium aluminium tetrahydride; sodium hydride; triethylamine; 9-bora-bicyclo[3.3.1]nonane; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;