2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane

Base Information

Chemical Name:2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane
CAS No.:1197820-00-0
Molecular Formula:C₃₆H₃₈O₆S
Molecular Weight:598.76
Hs Code.:

Synonyms:2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane

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Chemical Property of 2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane

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Technology Process of 2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane

There total 5 articles about 2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1197819-98-9
2-methoxy-2-(S)-phenyl-(1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane

: 100-39-0
benzyl bromide

: 1197820-00-0
2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane

Guidance literature:: 2-methoxy-2-(S)-phenyl-(1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 1.16667h; Inert atmosphere;

benzyl bromide; In N,N-dimethyl-formamide; oil; at 0 ℃; for 2.5h; Inert atmosphere;
DOI:10.1039/b913308a

Reference yield:

: 3254-12-4
2,3,4,6-tetra-O-acetyl-1-thio-β-D-glucopyranosyl acetophenone

: 1197820-00-0
2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / Inert atmosphere

2: toluene-4-sulfonic acid / Inert atmosphere

3: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

With sodium methylate; sodium hydride; toluene-4-sulfonic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.201101889

Reference yield:

: 1197819-96-7
C₁₄H₁₈O₆S

: 1197820-00-0
2-methoxy-2-(S)-phenyl-(3,4,6-tri-O-benzyl-1,2-dideoxy-β-D-glucopyranoso)[1,2-e]-1,4-oxathiane

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

With sodium hydride; toluene-4-sulfonic acid; In N,N-dimethyl-formamide;
DOI:10.1002/chem.201101889