diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate

Base Information

Chemical Name:diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate
CAS No.:1234628-01-3
Molecular Formula:C₂₉H₃₁O₆P
Molecular Weight:506.535
Hs Code.:

Synonyms:diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate

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Technology Process of diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate

There total 1 articles about diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: (5E,7E)-methyl 8-(3,5-dimethoxyphenyl)octa-5,7-dienoate

: 7526-26-3
diphenyl methylphosphonate

: 1234628-01-3
diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol101141a

Reference yield: 48.0%

: 842103-98-4
tert-butyl (2-methyl-3-oxopropyl)carbamate

: 1234628-01-3
diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate

: 1234627-95-2
tert-butyl ((3Z,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trien-1-yl)carbamate

: 1234627-91-8
tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate

Guidance literature:: diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate; With sodium iodide; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; at -78 - 0 ℃; Inert atmosphere;

tert-butyl (2-methyl-3-oxopropyl)carbamate; In tetrahydrofuran; at -78 - 0 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol101141a