tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate

Base Information

Chemical Name:tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate
CAS No.:1234627-91-8
Molecular Formula:C₂₆H₃₇NO₅
Molecular Weight:443.583
Hs Code.:

Synonyms:tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate

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Chemical Property of tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate

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Technology Process of tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate

There total 2 articles about tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1108750-53-3
dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate

: 842103-98-4
tert-butyl (2-methyl-3-oxopropyl)carbamate

: 1234627-95-2
tert-butyl ((3Z,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trien-1-yl)carbamate

: 1234627-91-8
tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate

Guidance literature:: dimethyl (6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dienylphosphonate; With N-ethyl-N,N-diisopropylamine; lithium chloride; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

tert-butyl (2-methyl-3-oxopropyl)carbamate; In acetonitrile; for 16h; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol101141a

Reference yield: 48.0%

: 842103-98-4
tert-butyl (2-methyl-3-oxopropyl)carbamate

: 1234628-01-3
diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate

: 1234627-95-2
tert-butyl ((3Z,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trien-1-yl)carbamate

: 1234627-91-8
tert-butyl (3E,9E,11E)-12-(3,5-dimethoxyphenyl)-2-methyl-5-oxododeca-3,9,11-trienylcarbamate

Guidance literature:: diphenyl ((6E,8E)-9-(3,5-dimethoxyphenyl)-2-oxonona-6,8-dien-1-yl)phosphonate; With sodium iodide; N,N,N',N'-tetramethylguanidine; In tetrahydrofuran; at -78 - 0 ℃; Inert atmosphere;

tert-butyl (2-methyl-3-oxopropyl)carbamate; In tetrahydrofuran; at -78 - 0 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol101141a