(2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione

Base Information

• Chemical Name: (2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione
• CAS No.: 259540-46-0
• Molecular Formula: C₄₂H₄₆N₄O₆
• Molecular Weight: 702.85

Synonyms:(2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione

Chemical Property of (2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione

There total 1 articles about (2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4R,5S)-1-(3-(3-methoxyphenyl)propanoyl)-3,4-dimethyl-5-phenyl-2-imidazolidinone → (2R,3S)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione (259540-47-1) + (2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione (259540-46-0)

Guidance literature:

With titanium tetrachloride; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 24h; Further Variations:; Reagents; reaction time; Product distribution;

DOI:10.1021/jo991317o

Reference yield:

(2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione (259540-46-0) → (2R,3R)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-diol

Guidance literature:

With lithium borohydride; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jo991317o

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) + (2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione (259540-46-0) → (4R,5S)-3,4-dimethyl-5-phenyl-imidazolidin-2-one (112791-04-5) + (CH2OCH2CH2C6H5)2(C2H4O2)2(SiC6H14)2

Guidance literature:

(2R,3R)-1,4-bis((4R,5S)-3,4-dimethyl-2-oxo-5-phenylimidazolidinyl)-2,3-bis[(3-methoxyphenyl)methyl]butane-1,4-dione; With lithium borohydride; In tetrahydrofuran; at 20 ℃;

tert-butyldimethylsilyl chloride; With 1H-imidazole; In N,N-dimethyl-formamide; Further stages.;

DOI:10.1021/jo991317o

Downstream raw materials:

(1R,2R)-1,2-bis[(3-methoxyphenyl)methyl]ethane-1,2-dicarboxylic acid

(4R,5S)-3,4-dimethyl-5-phenyl-imidazolidin-2-one

(2R,3R)-2,3-bis[(3,4-dimethoxyphenyl)methyl]butane-1,4-diol

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