cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan

Base Information

Chemical Name:cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan
CAS No.:960252-90-8
Molecular Formula:C₂₁H₂₀O₂
Molecular Weight:304.389
Hs Code.:

Synonyms:cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan

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Chemical Property of cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan

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Technology Process of cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan

There total 4 articles about cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 13922-41-3
1-Naphthylboronic acid

: 119646-68-3
3-bromo-5-tert-butyl-2-hydroxy-benzaldehyde

: 960252-90-8
cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan

Guidance literature:: With potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; at 90 ℃; for 13h;
DOI:10.1080/00397910701572423

Reference yield:

: 98-54-4
para-tert-butylphenol

: 960252-90-8
cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / bromine / CCl₄; CHCl₃ / 0 °C

2: 61 percent / Mg(OCH₃)2

3: 83 percent / potassium carbonate / Pd(PPh₃)4 / 1,2-dimethoxy-ethane; H₂O / 13 h / 90 °C

With bromine; potassium carbonate; magnesium methanolate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrachloromethane; 1,2-dimethoxyethane; chloroform; water; 3: Suzuki-Miyaura coupling;
DOI:10.1080/00397910701572423

Reference yield:

: 2198-66-5
2-bromo-4-tert-butylphenol

: 960252-90-8
cis-8-formyl-6a,11b-dihydro-10-(2,2-dimethylethyl)naphtho[2,1-b]benzo[d]furan

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / Mg(OCH₃)2

2: 83 percent / potassium carbonate / Pd(PPh₃)4 / 1,2-dimethoxy-ethane; H₂O / 13 h / 90 °C

With potassium carbonate; magnesium methanolate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; 2: Suzuki-Miyaura coupling;
DOI:10.1080/00397910701572423