N-(4'-azidobutyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin

Base Information

• Chemical Name: N-(4'-azidobutyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin
• CAS No.: 1448811-38-8
• Molecular Formula: C₃₈H₄₄N₄O₄
• Molecular Weight: 620.792
• Mol file: 1448811-38-8.mol

Synonyms:N-(4'-azidobutyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin

Chemical Property of N-(4'-azidobutyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4'-azidobutyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin

There total 1 articles about N-(4'-azidobutyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

toluenesulfonic acid 3-azidobutyl ester (389131-94-6) + [2R-(2α,3α,4α,5β)]-3,4,5-tris(phenylmethoxy)-2-[(phenylmethoxy)methyl]piperidine (167904-18-9) → N-(4'-azidobutyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin (1448811-38-8)

Guidance literature:

With potassium carbonate; In acetonitrile; at 85 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.bmc.2013.03.014

Reference yield: 66.0%

1-((prop-2-yn-1-yloxy)methyl)adamantane (547709-37-5) + N-(4'-azidobutyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin (1448811-38-8) → N-(4'-(4-(adamant-1-yl-methoxymethyl)-1H-1-2-3-triazol-1-yl)butyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin (1448811-39-9)

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; In dichloromethane; water; at 20 ℃; for 20h; Inert atmosphere;

DOI:10.1016/j.bmc.2013.03.014

upstream raw materials:

toluenesulfonic acid 3-azidobutyl ester

[2R-(2α,3α,4α,5β)]-3,4,5-tris(phenylmethoxy)-2-[(phenylmethoxy)methyl]piperidine

Downstream raw materials:

N-(4'-(4-(adamant-1-yl-methoxymethyl)-1H-1-2-3-triazol-1-yl)butyl)-2,3,4,6-tetra-O-benzyl-1-deoxygalactonojirimycin