N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)acetamidine

Base Information

• Chemical Name: N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)acetamidine
• CAS No.: 1060665-33-9
• Molecular Formula: C₂₅H₄₃N₂O₄P
• Molecular Weight: 466.601
• Mol file: 1060665-33-9.mol

Synonyms:N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)acetamidine

Chemical Property of N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)acetamidine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)acetamidine

There total 1 articles about N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)acetamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

ethyl N-benzoyl-2-(dibutoxyphosphoryl)ethanimidate + dibutylamine (111-92-2) → N1,N1-di(1-butyl)-N2-benzoyl(di(1-butoxy)phosphoryl)acetamidine (1060665-33-9)

Guidance literature:

at 50 - 60 ℃; for 3h; Neat (no solvent);

DOI:10.1134/S1070363210010093

Reference yield: 89.0%

N1,N1-di(1-butyl)-N2-benzoyl(di(1-butoxy)phosphoryl)acetamidine (1060665-33-9) + diethyl chlorophosphate (814-49-3) → N1,N1-dibutyl-N2-benzoyl-(2-diethoxyphosphoryl-2-dibutoxyphosphoryl)acetamidine (1283110-00-8)

Guidance literature:

N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)acetamidine; With sodium; In 1,4-dioxane; at 20 - 30 ℃;

diethyl chlorophosphate; In 1,4-dioxane; at 20 - 40 ℃;

DOI:10.1134/S1070363211040037

Reference yield: 88.0%

N1,N1-di(1-butyl)-N2-benzoyl(di(1-butoxy)phosphoryl)acetamidine (1060665-33-9) → N1,N1-di(1-butyl)-N2-benzoyl(di(1-butoxy)phosphoryl)bromoacetamidine (1060665-39-5)

Guidance literature:

N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)acetamidine; With sodium; In 1,4-dioxane; at 20 - 30 ℃;

With bromine; In 1,4-dioxane; at 20 - 30 ℃;

DOI:10.1134/S1070363210010093

upstream raw materials:

dibutylamine

Downstream raw materials:

N₁,N₁-di(1-butyl)-N₂-benzoyl(di(1-butoxy)phosphoryl)bromoacetamidine

N₁,N₁-dibutyl-N₂-benzoyl-(2-diethoxyphosphoryl-2-dibutoxyphosphoryl)acetamidine

N₁,N₁-dibutyl-N₂-benzoyl-(2-dimethoxyphosphoryl-2-dibutoxyphosphoryl)acetamidine

N,N-dibutyl-N'-benzoyl(trimethylsilyl)(dibutoxyphosphoryl)acetamidine