Technology Process of C16H16F2N6O4S2
There total 3 articles about C16H16F2N6O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium nitrate; sulfuric acid / water / -10 - 20 °C
2: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 10343.2 Torr / Autoclave
3: pyridine / dichloromethane / 16 h / 20 °C
4: hydrogenchloride / ethanol; water / 2 h / 80 °C
5: acetic acid / methanol / 2 h / 50 °C
6: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C
With
pyridine; hydrogenchloride; sulfuric acid; hydrogen; acetic acid; potassium nitrate; 3-chloro-benzenecarboperoxoic acid;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 10343.2 Torr / Autoclave
2: pyridine / dichloromethane / 16 h / 20 °C
3: hydrogenchloride / ethanol; water / 2 h / 80 °C
4: acetic acid / methanol / 2 h / 50 °C
5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 20 °C
With
pyridine; hydrogenchloride; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid;
palladium 10% on activated carbon;
In
methanol; ethanol; dichloromethane; water;