C₂₀H₃₄O₄Si

Base Information

Chemical Name:C₂₀H₃₄O₄Si
CAS No.:1360594-04-2
Molecular Formula:C₂₀H₃₄O₄Si
Molecular Weight:366.573
Hs Code.:

C<sub>20</sub>H<sub>34</sub>O<sub>4</sub>Si

Synonyms:C₂₀H₃₄O₄Si

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Chemical Property of C₂₀H₃₄O₄Si

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Technology Process of C₂₀H₃₄O₄Si

There total 10 articles about C₂₀H₃₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360594-03-1
(4R)-4-[2-(tert-butyldimethylsilyloxy)-5-(methoxymethoxy)-4-methylphenyl]pentan-1-ol

: 1360594-04-2
C₂₀H₃₄O₄Si

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃; for 0.5h;
DOI:10.1016/j.tetlet.2011.12.115

Reference yield:

: 1313708-40-5
4-(methoxymethoxy)-3-methylphenol

: 1360594-04-2
C₂₀H₃₄O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / benzene / 0.5 h / 0 - 20 °C

2: trimethylaluminum / hexane / 1 h / 20 °C

3: 1H-imidazole; dmap / dichloromethane / 0.5 h / 20 °C

4: palladium on activated charcoal; hydrogen / tetrahydrofuran / 15 h / 20 °C / 3800.26 Torr

5: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 0.5 h / -78 - 20 °C

With 1H-imidazole; dmap; oxalyl dichloride; tributylphosphine; palladium on activated charcoal; hydrogen; trimethylaluminum; dimethyl sulfoxide; triethylamine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; hexane; dichloromethane; benzene; 1: Mitsunobu coupling / 2: Claisen rearrangement / 5: Swern oxidation;
DOI:10.1016/j.tetlet.2011.12.115

Reference yield:

: 183623-25-8
C₁₂H₁₆O₂

: 1360594-04-2
C₂₀H₃₄O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1: tributylphosphine; 1,1'-azodicarbonyl-dipiperidine / benzene / 0.5 h / 0 - 20 °C

2: trimethylaluminum / hexane / 1 h / 20 °C

3: 1H-imidazole; dmap / dichloromethane / 0.5 h / 20 °C

4: palladium on activated charcoal; hydrogen / tetrahydrofuran / 15 h / 20 °C / 3800.26 Torr

5: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / 0.5 h / -78 - 20 °C

With 1H-imidazole; dmap; oxalyl dichloride; tributylphosphine; palladium on activated charcoal; hydrogen; trimethylaluminum; dimethyl sulfoxide; triethylamine; 1,1'-azodicarbonyl-dipiperidine; In tetrahydrofuran; hexane; dichloromethane; benzene; 1: Mitsunobu coupling / 2: Claisen rearrangement / 5: Swern oxidation;
DOI:10.1016/j.tetlet.2011.12.115