methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate

Base Information

Chemical Name:methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate
CAS No.:308803-68-1
Molecular Formula:C₂₂H₂₉NO₅
Molecular Weight:387.476
Hs Code.:

Synonyms:methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate

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Chemical Property of methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate

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Technology Process of methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate

There total 3 articles about methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 308803-66-9
(E)-methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethenyl]phenyl)ethyl]-N-methylcarbamate

: 308803-68-1
methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 2h; under 2068.59 - 2585.74 Torr;
DOI:10.1071/ch00023

Reference yield:

: 41498-37-7
7,12-O,O'-dimethylcoclaurine

: 308803-68-1
methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 2 h

1.2: 90 percent / NaBH₄ / methanol / 5 h

2.1: 64.8 percent / Et₃N / CHCl₃ / 5 h / 10 - 15 °C

3.1: 97 percent / H₂ / Pd/C (10 percent) / methanol / 2 h / 2068.59 - 2585.74 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; chloroform; 1.1: Eschweiler-Clark methylation;
DOI:10.1071/ch00023

Reference yield:

: 1934-93-6,13425-06-4
6,7-dimethoxy-1-(4-methoxybenzyl)-2-methyl-1,2,3,4-tetrahydroisoquinoline

: 308803-68-1
methyl N-[2-(4,5-dimethoxy-2-[2-(4-methoxyphenyl)ethyl]phenyl)ethyl]-N-methylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 64.8 percent / Et₃N / CHCl₃ / 5 h / 10 - 15 °C

2: 97 percent / H₂ / Pd/C (10 percent) / methanol / 2 h / 2068.59 - 2585.74 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1071/ch00023