adipic acid (3',5'-dimethoxybenzoin) ester methyl ester

Base Information

Chemical Name:adipic acid (3',5'-dimethoxybenzoin) ester methyl ester
CAS No.:457612-26-9
Molecular Formula:C₂₃H₂₆O₇
Molecular Weight:414.455
Hs Code.:

Synonyms:adipic acid (3',5'-dimethoxybenzoin) ester methyl ester

Suppliers and Price of adipic acid (3',5'-dimethoxybenzoin) ester methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of adipic acid (3',5'-dimethoxybenzoin) ester methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of adipic acid (3',5'-dimethoxybenzoin) ester methyl ester

There total 7 articles about adipic acid (3',5'-dimethoxybenzoin) ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5425-44-5
2-Phenyl-[1,3]dithiane

: 457612-26-9
adipic acid (3',5'-dimethoxybenzoin) ester methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-BuLi / tetrahydrofuran / 0.5 h / 0 °C

1.2: 100 percent / tetrahydrofuran / 1.5 h / 0 - 20 °C

2.1: 56 percent / bis(trifluoroacetoxy)iodobenzene / acetonitrile; H₂O / 1 h / 20 °C

3.1: 76 percent / 4-(N,N-dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CHCl₃ / 24 h / 60 °C

4.1: 87 percent Spectr_. / acetonitrile / 24 h / Irradiation; 419 nm irradiation

5.1: 5.6 mg / benzene; ethanol; hexane / 1 h

With dmap; n-butyllithium; dicyclohexyl-carbodiimide; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; ethanol; hexane; chloroform; water; acetonitrile; benzene;
DOI:10.1021/jo025837m

Reference yield:

: 34904-92-2
2-(3,5-dimethoxyphenyl)-2-hydroxy-1-phenylethan-1-one

: 457612-26-9
adipic acid (3',5'-dimethoxybenzoin) ester methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / 4-(N,N-dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CHCl₃ / 24 h / 60 °C

2: 87 percent Spectr_. / acetonitrile / 24 h / Irradiation; 419 nm irradiation

3: 5.6 mg / benzene; ethanol; hexane / 1 h

With dmap; dicyclohexyl-carbodiimide; In ethanol; hexane; chloroform; acetonitrile; benzene;
DOI:10.1021/jo025837m

Reference yield:

: 100-52-7
benzaldehyde

: 457612-26-9
adipic acid (3',5'-dimethoxybenzoin) ester methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1.1: 62 percent / methanol; acetyl chloride / CH₂Cl₂ / 3 h / 20 °C

2.1: n-BuLi / tetrahydrofuran / 0.5 h / 0 °C

2.2: 100 percent / tetrahydrofuran / 1.5 h / 0 - 20 °C

3.1: 56 percent / bis(trifluoroacetoxy)iodobenzene / acetonitrile; H₂O / 1 h / 20 °C

4.1: 76 percent / 4-(N,N-dimethylamino)pyridine; N,N'-dicyclohexylcarbodiimide / CHCl₃ / 24 h / 60 °C

5.1: 87 percent Spectr_. / acetonitrile / 24 h / Irradiation; 419 nm irradiation

6.1: 5.6 mg / benzene; ethanol; hexane / 1 h

With methanol; dmap; n-butyllithium; acetyl chloride; dicyclohexyl-carbodiimide; bis-[(trifluoroacetoxy)iodo]benzene; In tetrahydrofuran; ethanol; hexane; dichloromethane; chloroform; water; acetonitrile; benzene;
DOI:10.1021/jo025837m