(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) (trimethylsilylacetylenyl)

Base Information

• Chemical Name: (((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) (trimethylsilylacetylenyl)
• CAS No.: 854669-44-6
• Molecular Formula: C₄₀H₆₂FeN₂Si
• Molecular Weight: 654.878

Synonyms:(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) (trimethylsilylacetylenyl)

Chemical Property of (((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) (trimethylsilylacetylenyl)

Chemical Property:

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Technology Process of (((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) (trimethylsilylacetylenyl)

There total 2 articles about (((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) (trimethylsilylacetylenyl) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

(((2,6-di(isopropyl)phenyl)N)2C3H-t-Bu2 iron(II) fluoride (854669-27-5) + Bis(trimethylsilyl)ethyne (14630-40-1) → (((2,6-di(isopropyl)phenyl)N)2C3H-t-Bu2 iron(II) (trimethylsilylacetylenyl) (854669-44-6)

Guidance literature:

In diethyl ether; byproducts: (CH3)3SiF; (N2), 2 equiv. of ligand added to Fe complex in Et2O under stirring; crystd. at -38°C, elem. anal.;

DOI:10.1021/ja042672l

Reference yield:

[Fe(methyl)(2,2,6,6-tetramethyl-3,5-bis(2,6-diisopropylphenylimido)hept-4-yl)] (415701-49-4) → (((2,6-di(isopropyl)phenyl)N)2C3H-t-Bu2 iron(II) (trimethylsilylacetylenyl) (854669-44-6)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene

2: diethyl ether

In diethyl ether; toluene;

DOI:10.1021/ja042672l

upstream raw materials:

(((2,6-di(isopropyl)phenyl)N)2C₃H-t-Bu₂ iron(II) fluoride

Bis(trimethylsilyl)ethyne

[Fe(methyl)(2,2,6,6-tetramethyl-3,5-bis(2,6-diisopropylphenylimido)hept-4-yl)]

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