1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane

Base Information

Chemical Name:1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane
CAS No.:200863-79-2
Molecular Formula:C₃₀H₄₆O₁₀
Molecular Weight:566.689
Hs Code.:

Synonyms:1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane

Chemical Property:

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Technology Process of 1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane

There total 4 articles about 1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 107-30-2
chloromethyl methyl ether

: 200863-76-9
1,8-Bis-(5-methoxy-2-methoxymethoxy-phenyl)-octane-1,8-diol

: 200863-79-2
1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 5h; Ambient temperature;
DOI:10.1016/S0040-4020(97)10196-X

Reference yield:

: 672-13-9
2-hydroxy-5-methoxybenzaldehyde

: 200863-79-2
1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / diisopropyl ethylamine / CH₂Cl₂ / 4 h / Ambient temperature

2: 1.) Mg, I₂ / 1.) THF, reflux, 1.5 h, 2.) THF, room temperature, 3 h

3: 100 percent / diisopropyl ethylamine / CH₂Cl₂ / 5 h / Ambient temperature

With iodine; magnesium; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4020(97)10196-X

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 200863-79-2
1,8-bis(2-methoxymethyloxy-5-methoxyphenyl)-1,8-dimethoxymethyloxyoctane

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Mg, I₂ / 1.) THF, reflux, 1.5 h, 2.) THF, room temperature, 3 h

2: 100 percent / diisopropyl ethylamine / CH₂Cl₂ / 5 h / Ambient temperature

With iodine; magnesium; N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/S0040-4020(97)10196-X