Technology Process of C64H54O9
There total 9 articles about C64H54O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1055/s-0028-1087371
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 3h;
DOI:10.3987/COM-15-S(T)25
- Guidance literature:
-
Multi-step reaction with 5 steps
1: iodine / chloroform / 25 h / 20 °C / Inert atmosphere
2: Oxone; potassium carbonate; tetra(n-butyl)ammonium hydrogensulfate; (5S,8R,9R)-2,2-dimethyl-10-oxo-1,3,6-trioxaspiro[4.5]decane-8,9-diyl diacetate / acetonitrile; aq. phosphate buffer / 0.42 h / 0 °C / pH 9.18
3: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.17 h / 0 °C
4: camphor-10-sulfonic acid / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 3 h / 20 °C
With
(5S,8R,9R)-2,2-dimethyl-10-oxo-1,3,6-trioxaspiro[4.5]decane-8,9-diyl diacetate; dmap; Oxone; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; iodine; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
tetrahydrofuran; aq. phosphate buffer; dichloromethane; chloroform; acetonitrile;
DOI:10.3987/COM-15-S(T)25
