1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane

Base Information

• Chemical Name: 1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane
• CAS No.: 444584-68-3
• Molecular Formula: C₃₀H₃₄Cl₂N₂Si₂
• Molecular Weight: 549.69

Synonyms:1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane

Chemical Property of 1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane

Chemical Property:

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Technology Process of 1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane

There total 4 articles about 1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

hexakis[2-(dimethylaminomethyl)phenyl]cyclotrisilane (143504-44-3) + diphenylsilyl dichloride (80-10-4) → 1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane (444584-68-3)

Guidance literature:

In toluene; at 55 ℃; for 48h;

DOI:10.1016/S0022-328X(01)01451-6

Reference yield:

diphenylsilyl dichloride (80-10-4) + 1,3-dichloro-1,1,3,3-tetrakis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyltrisilane (444584-84-3) → 1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane (444584-68-3)

Guidance literature:

In benzene-d6; at 70 ℃; for 18h;

DOI:10.1016/S0022-328X(01)01451-6

Reference yield:

2,3-dimethyl-buta-1,3-diene (513-81-5) + 1,3-dichloro-1,1,3,3-tetrakis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyltrisilane (444584-84-3) → bis<<2-(N,N-dimethylamino)methyl>phenyl>3,4-dimethylsilacyclopent-3-ene + 1,2-dichloro-1,1-bis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyldisilane (444584-68-3)

Guidance literature:

In benzene-d6; at 70 ℃; for 18h;

DOI:10.1016/S0022-328X(01)01451-6

upstream raw materials:

2,3-dimethyl-buta-1,3-diene

1,3-dichloro-1,1,3,3-tetrakis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyltrisilane

hexakis[2-(dimethylaminomethyl)phenyl]cyclotrisilane

diphenylsilyl dichloride

Downstream raw materials:

1,3-dichloro-1,1,3,3-tetrakis[2-(dimethylaminomethyl)phenyl]-2,2-diphenyltrisilane

diphenylsilyl dichloride

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