para-toluenesulphonic acid efinaconazole salt

Base Information

Chemical Name:para-toluenesulphonic acid efinaconazole salt
CAS No.:164650-61-7
Molecular Formula:C₇H₈O₃S*C₁₈H₂₂F₂N₄O
Molecular Weight:520.6
Hs Code.:

Synonyms:para-toluenesulphonic acid efinaconazole salt

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Chemical Property of para-toluenesulphonic acid efinaconazole salt

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Technology Process of para-toluenesulphonic acid efinaconazole salt

There total 3 articles about para-toluenesulphonic acid efinaconazole salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 104-15-4
toluene-4-sulfonic acid

: 164650-45-7,164650-44-6
(2R,3R)-2-(2,4-difluorophenyl)-3-(4-methylenepiperidine-1-yl)-1-(1H-1,2,4-triazole-1-yl)-butane-2-ol

: 164650-61-7
para-toluenesulphonic acid efinaconazole salt

Guidance literature:: In isopropyl alcohol; at 70 ℃; for 3h; Inert atmosphere;

Reference yield:

: 3522-98-3
4-methylenepiperidine hydrobromide

: (2R,3S)-2-(2,4-difluorophenyl)-3-methyl-2-[(1H-1,2,4-triazolyl)methyl]oxirane

: 104-15-4
toluene-4-sulfonic acid

: 164650-61-7
para-toluenesulphonic acid efinaconazole salt

Guidance literature:: 4-methylenepiperidine hydrobromide; (2R,3S)-2-(2,4-difluorophenyl)-3-methyl-2-[(1H-1,2,4-triazolyl)methyl]oxirane; With lithium nitrate; N,N,N',N'-tetramethylguanidine; In acetonitrile; for 30h; Inert atmosphere; Reflux;

toluene-4-sulfonic acid; In isopropyl alcohol; at 70 ℃; for 3h;