(2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol

Base Information

Chemical Name:(2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol
CAS No.:154659-19-5
Molecular Formula:C₃₁H₄₇NO₅
Molecular Weight:513.718
Hs Code.:

(2S,3R,4R)-1-(benzyloxy)-2-<N-(benzyloxycarbonyl)amino>hexadecane-3,4-diol

Synonyms:(2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol

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Chemical Property of (2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol

Chemical Property:

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Technology Process of (2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol

There total 4 articles about (2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58577-87-0
O-benzyl-L-serinol

: 154659-19-5
(2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / tetrahydrofuran; H₂O / 2.17 h / 0 - 20 °C

2: 1.) DMSO, COCl₂, 2.) Et₃N / 1.) CH₂Cl₂, -63 deg C, 20 min, 2.) CH₂Cl₂, -63 deg C, 20 min

With potassium carbonate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; water;
DOI:10.1021/ja00083a017

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 154659-19-5
(2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / tetrahydrofuran; H₂O / 2.17 h / 0 - 20 °C

2: 1.) DMSO, COCl₂, 2.) Et₃N / 1.) CH₂Cl₂, -63 deg C, 20 min, 2.) CH₂Cl₂, -63 deg C, 20 min

With potassium carbonate; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; water;
DOI:10.1021/ja00083a017

Reference yield:

: 58578-42-0,98757-96-1,58577-90-5
(R)-benzyl 1-(benzyloxy)-3-hydroxypropan-2-ylcarbamate

: 154659-19-5
(2S,3R,4R)-1-(benzyloxy)-2-hexadecane-3,4-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) DMSO, COCl₂, 2.) Et₃N / 1.) CH₂Cl₂, -63 deg C, 20 min, 2.) CH₂Cl₂, -63 deg C, 20 min

With dimethyl sulfoxide; triethylamine;
DOI:10.1021/ja00083a017