3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride

Base Information

Chemical Name:3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride
CAS No.:87286-86-0
Molecular Formula:C₂₆H₂₅Cl₂NO₆
Molecular Weight:518.394
Hs Code.:

Synonyms:3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride

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Chemical Property of 3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride

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Technology Process of 3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride

There total 4 articles about 3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 87286-85-9
3-[3-(2-Carboxy-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionic acid

: 87286-86-0
3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride

Guidance literature:: With oxalyl dichloride; In pyridine; benzene; 1.) 15 h, r.t.; 2.) 5 h, 50 deg C;
DOI:10.1002/hlca.19830660411

Reference yield:

: 4808-48-4
2,3-diphenylmaleic anhydride

: 87286-86-0
3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / dimethylformamide; toluene / 12 h / Heating

2: 17 percent / Na, conc. H₂SO₄ / benzene

3: 77 percent / conc. H₂SO₄ / 50 h / Ambient temperature

4: 98 percent / oxalyl chloride / pyridine; benzene / 1.) 15 h, r.t.; 2.) 5 h, 50 deg C

With oxalyl dichloride; sulfuric acid; sodium; In pyridine; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1002/hlca.19830660411

Reference yield:

: 87309-51-1
N-(1,3-Dihydroxy-2-methyl-2-propyl)-2,3-diphenyl-maleinimid

: 87286-86-0
3-[3-(2-Chlorocarbonyl-ethoxy)-2-(2,5-dioxo-3,4-diphenyl-2,5-dihydro-pyrrol-1-yl)-2-methyl-propoxy]-propionyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: 17 percent / Na, conc. H₂SO₄ / benzene

2: 77 percent / conc. H₂SO₄ / 50 h / Ambient temperature

3: 98 percent / oxalyl chloride / pyridine; benzene / 1.) 15 h, r.t.; 2.) 5 h, 50 deg C

With oxalyl dichloride; sulfuric acid; sodium; In pyridine; benzene;
DOI:10.1002/hlca.19830660411