(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate

Base Information

Chemical Name:(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate
CAS No.:439610-90-9
Molecular Formula:C₃₉H₄₄O₆
Molecular Weight:608.775
Hs Code.:

Synonyms:(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate

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Chemical Property of (S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate

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Technology Process of (S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate

There total 14 articles about (S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4541-14-4
4-benzyloxy-butan-1-ol

: 439610-90-9
(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine / CH₂Cl₂ / 0 - 5 °C

2.1: K₂CO₃ / acetone / 192 h / Heating

2.2: KOH / ethane-1,2-diol / 4 h / Heating

3.1: oxalyl chloride; N,N-dimethylformamide / toluene / 40 - 45 °C

4.1: 4-dimethylaminopyridine; pyridine / toluene / 16 h / 40 - 45 °C

With pyridine; dmap; oxalyl dichloride; potassium carbonate; N,N-dimethyl-formamide; In dichloromethane; acetone; toluene;

Reference yield:

: 1486-51-7
p-(benzyloxy)benzoic acid

: 439610-90-9
(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride; N,N-dimethylformamide / toluene / 40 - 45 °C

2: 30.9 g / 4-dimethylaminopyridine; pyridine / toluene / 16 h / 40 - 45 °C

3: 94 percent / H₂ / Pd/C / tetrahydrofuran

4: 4-dimethylaminopyridine; pyridine / toluene / 16 h / 40 - 45 °C

With pyridine; dmap; oxalyl dichloride; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; toluene;

Reference yield:

: 111153-20-9
(S)-(+)-1-methylheptyl 4-benzyloxybenzoate

: 439610-90-9
(S)-(+)-4-(1-methylheptyloxycarbonyl)phenyl 4-(4-benzyloxybut-1-oxy)biphenyl-4'-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / H₂ / Pd/C / tetrahydrofuran

2: 4-dimethylaminopyridine; pyridine / toluene / 16 h / 40 - 45 °C

With pyridine; dmap; hydrogen; palladium on activated charcoal; In tetrahydrofuran; toluene;