(S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate

Base Information

• Chemical Name: (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate
• CAS No.: 1072841-05-4
• Molecular Formula: C₂₁H₂₄N₄O₄
• Molecular Weight: 396.446

Synonyms:(S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate

Chemical Property of (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate

Chemical Property:

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Technology Process of (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate

There total 3 articles about (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

1,2,3-Benzotriazole (95-14-7,27556-51-0) + BOC-O-benzyl-L-serine (23680-31-1) → (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate (1072841-05-4)

Guidance literature:

BOC-O-benzyl-L-serine; With dicyclohexyl-carbodiimide; In dichloromethane; for 0.5h; Inert atmosphere;

1,2,3-Benzotriazole; In dichloromethane; at 25 ℃; for 12h; Inert atmosphere;

DOI:10.1039/c3cc39291k

Reference yield:

BOC-O-benzyl-L-serine (23680-31-1) + 1-(methanesulfonyl)-1H-1,2,3-benzotriazole (37073-15-7) → (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate (1072841-05-4)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 50 ℃; Microwave irradiation;

DOI:10.1111/cbdd.12134

Reference yield:

1,2,3-Benzotriazole (95-14-7,27556-51-0) + C15H20ClNO4 → (S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate (1072841-05-4)

Guidance literature:

DOI:10.3184/030823407X272985

upstream raw materials:

1,2,3-Benzotriazole

BOC-O-benzyl-L-serine

1-(methanesulfonyl)-1H-1,2,3-benzotriazole

Downstream raw materials:

N-(tert-butyloxycarbonyl)-O-benzyl-L-serinol

(S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

(S)-1-((S)-2-((S)-2-((S)-1-((6S,9S,12S)-9-((benzyloxy)methyl)-6,12-di((S)-sec-butyl)-2,2-dimethyl-4,7,10-trioxo-3-oxa-5,8,11-triazatridecan-13-oyl)pyrrolidine-2-carboxamido)-4-methylpentanamido)-3-phenylpropanoyl)pyrrolidine-2-carboxylic acid

(2S,3S)-1-(((S)-3-(benzyloxy)-1-(((2S,3S)-1-((S)-2-(((S)-1-(((S)-1-((S)-2-carboxypyrrolidin-1-yl)-1-oxo-3-phenylpropan-2-yl)amino)-4-methyl-1-oxopentan-2-yl)carbamoyl)pyrrolidin-1-yl)-3-methyl-1-oxopentan-2-yl)amino)-1-oxopropan-2-yl)amino)-3-methyl-1-oxopentan-2-aminium chloride

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