(S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

Base Information

Chemical Name:(S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride
CAS No.:1427166-54-8
Molecular Formula:C₁₆H₂₄N₂O₄*ClH
Molecular Weight:344.838
Hs Code.:

Synonyms:(S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

Suppliers and Price of (S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

There total 3 articles about (S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1427166-49-1
(2S,3S)-2-((S)-3-(benzyloxy)-2-((tert-butoxycarbonyl)amino)propanamido)-3-methylpentanoic acid

: 1427166-54-8
(S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 25 ℃; for 3h;
DOI:10.1039/c3cc39291k

Reference yield:

: 1072841-05-4
(S)-tert-butyl (1-(1H-benzo[d][1,2,3]triazol-1-yl)-3-(benzyloxy)-1-oxopropan-2-yl)carbamate

: 1427166-54-8
(S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / acetonitrile; water / 16 h

2: hydrogenchloride / 1,4-dioxane / 3 h / 25 °C

With hydrogenchloride; triethylamine; In 1,4-dioxane; water; acetonitrile;
DOI:10.1039/c3cc39291k

Reference yield:

: 23680-31-1
BOC-O-benzyl-L-serine

: 1427166-54-8
(S)-3-(benzyloxy)-1-(((1S,2S)-1-carboxy-2-methylbutyl)amino)-1-oxopropan-2-aminium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: dicyclohexyl-carbodiimide / dichloromethane / 0.5 h / Inert atmosphere

1.2: 12 h / 25 °C / Inert atmosphere

2.1: triethylamine / acetonitrile; water / 16 h

3.1: hydrogenchloride / 1,4-dioxane / 3 h / 25 °C

With hydrogenchloride; triethylamine; dicyclohexyl-carbodiimide; In 1,4-dioxane; dichloromethane; water; acetonitrile;
DOI:10.1039/c3cc39291k