C₅₁H₄₄N₁₂O₃

Base Information

Chemical Name:C₅₁H₄₄N₁₂O₃
CAS No.:1612874-03-9
Molecular Formula:C₅₁H₄₄N₁₂O₃
Molecular Weight:872.989
Hs Code.:

C<sub>51</sub>H<sub>44</sub>N<sub>12</sub>O<sub>3</sub>

Synonyms:C₅₁H₄₄N₁₂O₃

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Chemical Property of C₅₁H₄₄N₁₂O₃

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Technology Process of C₅₁H₄₄N₁₂O₃

There total 10 articles about C₅₁H₄₄N₁₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1612874-02-8
C₄₆H₄₁N₁₁O₄

: 62-53-3
aniline

: 1612874-03-9
C₅₁H₄₄N₁₂O₃

Guidance literature:: aniline; With trimethylaluminum; In toluene; at 20 ℃;

C₄₆H₄₁N₁₁O₄; In toluene; at 20 - 100 ℃; for 2h;
DOI:10.1002/ejoc.201301838

Reference yield:

: 6310-19-6
4-tert-butyl-2-nitroaniline

: 1612874-03-9
C₅₁H₄₄N₁₂O₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: Iodine monochloride / 1,2-dichloro-ethane / 3 h / 70 °C / Inert atmosphere

2.1: sodium nitrite; sulfuric acid / ethanol / 0 °C / Reflux

3.1: tin(II) chloride dihdyrate; ethanol / Reflux

4.1: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

5.1: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(ll) sulfate pentahydrate / ethanol; water / 12 h / 20 °C

6.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

6.2: 0.5 h

7.1: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate / water; tetrahydrofuran / 12 h / 20 °C

8.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

8.2: 0.5 h

9.1: copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 5 h / 20 °C

10.1: trimethylaluminum / toluene / 20 °C

10.2: 2 h / 20 - 100 °C

With copper(l) iodide; sodium azide; copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; sulfuric acid; trimethylaluminum; Iodine monochloride; copper(II) sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; N,N`-dimethylethylenediamine; sodium nitrite; In tetrahydrofuran; ethanol; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; toluene;
DOI:10.1002/ejoc.201301838

Reference yield:

: 1369827-82-6
C₁₀H₁₂INO₂

: 1612874-03-9
C₅₁H₄₄N₁₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: tin(II) chloride dihdyrate; ethanol / Reflux

2.1: sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(l) iodide; N,N`-dimethylethylenediamine / dimethyl sulfoxide; water / 1 h / 20 °C

3.1: sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; copper(II) sulfate / water; tetrahydrofuran / 12 h / 20 °C

4.1: dicyclohexyl-carbodiimide / dichloromethane / 0.17 h

4.2: 0.5 h

5.1: copper(l) iodide; 1,8-diazabicyclo[5.4.0]undec-7-ene / toluene / 5 h / 20 °C

6.1: trimethylaluminum / toluene / 20 °C

6.2: 2 h / 20 - 100 °C

With copper(l) iodide; sodium azide; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tin(II) chloride dihdyrate; ethanol; trimethylaluminum; copper(II) sulfate; 1,8-diazabicyclo[5.4.0]undec-7-ene; dicyclohexyl-carbodiimide; N,N`-dimethylethylenediamine; In tetrahydrofuran; dichloromethane; water; dimethyl sulfoxide; toluene;
DOI:10.1002/ejoc.201301838