C₂₅H₂₇NO₆

Base Information

Chemical Name:C₂₅H₂₇NO₆
CAS No.:1265173-12-3
Molecular Formula:C₂₅H₂₇NO₆
Molecular Weight:437.492
Hs Code.:

C<sub>25</sub>H<sub>27</sub>NO<sub>6</sub>

Synonyms:C₂₅H₂₇NO₆

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Chemical Property of C₂₅H₂₇NO₆

Chemical Property:

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Technology Process of C₂₅H₂₇NO₆

There total 22 articles about C₂₅H₂₇NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1196704-26-3
C₂₅H₃₁NO₆

: 1265173-12-3
C₂₅H₂₇NO₆

Guidance literature:: With Jones reagent; In water; acetone; at 0 - 20 ℃;
DOI:10.1002/asia.201000602

Reference yield:

: 1265173-20-3
C₂₂H₂₈O₇S

: 1265173-12-3
C₂₅H₂₇NO₆

Guidance literature:: Multi-step reaction with 14 steps

1.1: acetic anhydride; dimethyl sulfoxide / 2 h / 50 °C

2.1: toluene / 4 h / -40 °C

3.1: magnesium / methanol / 2 h / 20 °C

4.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C

5.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C

5.2: 0 - 20 °C

6.1: pyridine / dichloromethane / 2 h / 0 °C

7.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

8.1: dichloromethane / 1 h / 0 °C

9.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C

10.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

11.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

13.1: scandium tris(trifluoromethanesulfonate) / dichloromethane; water / 20 - 40 °C

14.1: Jones reagent / water; acetone / 0 - 20 °C

With pyridine; Jones reagent; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; acetic anhydride; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; acetone; toluene; mineral oil; 4.1: Swern oxidation / 5.2: Horner-Wadsworth-Emmons olefination / 9.1: Overman rearrangement;
DOI:10.1002/asia.201000602

Reference yield:

: 1265173-03-2
C₂₂H₂₆O₇S

: 1265173-12-3
C₂₅H₂₇NO₆

Guidance literature:: Multi-step reaction with 13 steps

1.1: toluene / 4 h / -40 °C

2.1: magnesium / methanol / 2 h / 20 °C

3.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / 4 h / 20 °C

4.1: sodium hydride / tetrahydrofuran; hexane; mineral oil / 0.17 h / 0 °C

4.2: 0 - 20 °C

5.1: pyridine / dichloromethane / 2 h / 0 °C

6.1: diisobutylaluminium hydride / toluene / 0.5 h / -78 °C

7.1: dichloromethane / 1 h / 0 °C

8.1: sodium carbonate / tert-butylbenzene / 24 h / 170 °C

9.1: diisobutylaluminium hydride / toluene / 1 h / -78 °C

10.1: potassium carbonate / tetrahydrofuran; water / 3 h / 0 °C

11.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.17 h / 0 °C

12.1: scandium tris(trifluoromethanesulfonate) / dichloromethane; water / 20 - 40 °C

13.1: Jones reagent / water; acetone / 0 - 20 °C

With pyridine; Jones reagent; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; sodium carbonate; potassium carbonate; magnesium; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; methanol; tert-butylbenzene; hexane; dichloromethane; water; acetone; toluene; mineral oil; 3.1: Swern oxidation / 4.2: Horner-Wadsworth-Emmons olefination / 8.1: Overman rearrangement;
DOI:10.1002/asia.201000602