ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate

Base Information

Chemical Name:ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate
CAS No.:1413644-32-2
Molecular Formula:C₂₈H₄₄N₂O₆
Molecular Weight:504.667
Hs Code.:

Synonyms:ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate

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Chemical Property of ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate

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Technology Process of ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate

There total 5 articles about ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 141903-93-7
(8Z)-heptadec-8-en-1-amine

: 530-62-1
1,1'-carbonyldiimidazole

: 412317-99-8
3-hydroxymethyl-4-nitrobenzoic acid ethyl ester

: 1413644-32-2
ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate

Guidance literature:: 1,1'-carbonyldiimidazole; 3-hydroxymethyl-4-nitrobenzoic acid ethyl ester; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;

(8Z)-heptadec-8-en-1-amine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo301659c

Reference yield:

: 916791-27-0
3-(bromomethyl)-4-nitrobenzoicacid

: 1413644-32-2
ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium carbonate / water; acetone / 12 h / Reflux

1.2: pH 2

2.1: boron trifluoride diethyl etherate / 5 h / Reflux

3.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; sodium carbonate; In dichloromethane; water; acetone;
DOI:10.1021/jo301659c

Reference yield:

: 914777-97-2
3-hydroxymethyl-4-nitrobenzoic acid

: 1413644-32-2
ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: boron trifluoride diethyl etherate / 5 h / Reflux

2.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1021/jo301659c