ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid

Base Information

Chemical Name:ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid
CAS No.:1413644-28-6
Molecular Formula:C₂₆H₄₀N₂O₆
Molecular Weight:476.613
Hs Code.:

Synonyms:ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid

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Chemical Property of ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid

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Technology Process of ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid

There total 6 articles about ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1413644-32-2
ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate

: 1413644-28-6
ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid

Guidance literature:: ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoate; With lithium hydroxide; In ethanol; water; at 20 ℃; for 12h;

With hydrogenchloride; In water; pH=2;
DOI:10.1021/jo301659c

Reference yield:

: 916791-27-0
3-(bromomethyl)-4-nitrobenzoicacid

: 1413644-28-6
ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / water; acetone / 12 h / Reflux

1.2: pH 2

2.1: boron trifluoride diethyl etherate / 5 h / Reflux

3.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

3.2: 20 °C / Inert atmosphere

4.1: lithium hydroxide / ethanol; water / 12 h / 20 °C

4.2: pH 2

With boron trifluoride diethyl etherate; sodium carbonate; lithium hydroxide; In ethanol; dichloromethane; water; acetone;
DOI:10.1021/jo301659c

Reference yield:

: 914777-97-2
3-hydroxymethyl-4-nitrobenzoic acid

: 1413644-28-6
ethyl 3-[[[(8Z)-heptadec-8-en-1-ylcarbamoyl]oxy]methyl]-4-nitrobenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: boron trifluoride diethyl etherate / 5 h / Reflux

2.1: dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: lithium hydroxide / ethanol; water / 12 h / 20 °C

3.2: pH 2

With boron trifluoride diethyl etherate; lithium hydroxide; In ethanol; dichloromethane; water;
DOI:10.1021/jo301659c