methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate

Base Information

Chemical Name:methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate
CAS No.:936636-01-0
Molecular Formula:C₁₇H₂₀N₂O₃
Molecular Weight:300.357
Hs Code.:

Synonyms:methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate

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Chemical Property of methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate

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Technology Process of methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate

There total 3 articles about methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 936636-00-9
methyl 4-(2-oxo-1,2-dihydropyridin-3-yl)benzoate

: 4584-46-7
(2-chloroethyl)dimethylamine hydrochloride

: 936636-01-0
methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate

Guidance literature:: methyl 4-(2-oxo-1,2-dihydropyridin-3-yl)benzoate; (2-chloroethyl)dimethylamine hydrochloride; With sodium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 7h;

With potassium carbonate; In N,N-dimethyl-formamide; for 2h;

Reference yield:

: 90395-47-4
methyl 4-(3-pyridinyl)benzoate

: 936636-01-0
methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: dihydrogen peroxide; acetic acid / water / 18 h / 70 °C

2.1: acetic anhydride / 24 h / 130 °C

3.1: sodium carbonate / N,N-dimethyl-formamide / 7 h / 80 °C

3.2: 2 h

With dihydrogen peroxide; acetic anhydride; sodium carbonate; acetic acid; In water; N,N-dimethyl-formamide;

Reference yield:

: 328125-44-6
methyl 4-[pyridine-N-oxide-3-yl]-benzoate

: 936636-01-0
methyl 4-{1-[2-(dimethylamino)ethyl]-2-oxo-1,2-dihydropyridin-3-yl}benzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 24 h / 130 °C

2.1: sodium carbonate / N,N-dimethyl-formamide / 7 h / 80 °C

2.2: 2 h

With acetic anhydride; sodium carbonate; In N,N-dimethyl-formamide;