3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone

Base Information

Chemical Name:3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone
CAS No.:1334242-06-6
Molecular Formula:C₂₁H₂₇N₃O₄S
Molecular Weight:417.529
Hs Code.:

Synonyms:3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone

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Chemical Property of 3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone

Chemical Property:

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Technology Process of 3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone

There total 4 articles about 3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.3%

: 1334242-04-4
3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfoxide

: 1334242-06-6
3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone

Guidance literature:: With Oxone; In methanol; water; at -10 - 20 ℃;
DOI:10.1016/j.ejmech.2013.01.054

Reference yield:

: 109-09-1
2-chloropyridine

: 1334242-06-6
3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone

Guidance literature:: Multi-step reaction with 6 steps

1.1: 15 h / 160 °C / Inert atmosphere

2.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere

2.2: 80 °C / Inert atmosphere

3.1: tetrahydrofuran / 0.17 h / Cooling with ice

4.1: tetrahydrofuran / 0.17 h / Cooling with ice

4.2: 0 - 20 °C

5.1: Oxone / methanol; water / -10 - -5 °C

6.1: Oxone / methanol; water / -10 - 20 °C

With Oxone; sodium hydride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2013.01.054

Reference yield:

: 122321-04-4
2-(N-methyl-N-(pyridin-2-yl)amino)ethanol

: 1334242-06-6
3-butyl-2-(4-(2-(methyl(pyridin-2-yl)amino)ethoxy)phenyl)thiazolidin-4-one sulfone

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h / Inert atmosphere

1.2: 80 °C / Inert atmosphere

2.1: tetrahydrofuran / 0.17 h / Cooling with ice

3.1: tetrahydrofuran / 0.17 h / Cooling with ice

3.2: 0 - 20 °C

4.1: Oxone / methanol; water / -10 - -5 °C

5.1: Oxone / methanol; water / -10 - 20 °C

With Oxone; sodium hydride; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.ejmech.2013.01.054