N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester

Base Information

Chemical Name:N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester
CAS No.:144412-02-2
Molecular Formula:C₂₉H₃₀N₄O₆
Molecular Weight:530.58
Hs Code.:

Synonyms:N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester

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Chemical Property of N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester

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Technology Process of N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester

There total 7 articles about N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15535-95-2
4-(aminoiminomethyl)benzoic acid

: 144412-02-2
N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / tetrahydrofuran; dimethylformamide / 20 °C

2: NaHCO₃ / CH₂Cl₂; H₂O

3: aq. Na₂CO₃ / CH₂Cl₂ / 2 h

With thionyl chloride; sodium hydrogencarbonate; sodium carbonate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00101a017

Reference yield:

: 14529-00-1
benzyl 3-aminopropionate

: 144412-02-2
N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.)2-chloro-4,6-dimethoxy-1,3,5-triazine (CDMT), N-methylmorpholine (NMM), 2.) N-methylmorpholine (NMM) / 1.) CH₂Cl₂, 0 deg C, 3 h, 2.) CH₂Cl₂, RT, 12 h

2: trifluoroacetic acid (TFA) / CH₂Cl₂ / 2 h / Ambient temperature

3: NaHCO₃ / CH₂Cl₂; H₂O

4: aq. Na₂CO₃ / CH₂Cl₂ / 2 h

With 4-methyl-morpholine; 2-chloro-4,6-dimethoxy-1 ,3,5-triazine; sodium hydrogencarbonate; sodium carbonate; trifluoroacetic acid; In dichloromethane; water;
DOI:10.1021/jm00101a017

Reference yield:

: 138108-38-0
3-(3-Amino-propionylamino)-propionic acid benzyl ester

: 144412-02-2
N-[N-[p-[N-(benzyloxycarbonyl)amidino]benzoyl]-β-alanyl]-β-alanine benzylester

Guidance literature:: Multi-step reaction with 2 steps

1: NaHCO₃ / CH₂Cl₂; H₂O

2: aq. Na₂CO₃ / CH₂Cl₂ / 2 h

With sodium hydrogencarbonate; sodium carbonate; In dichloromethane; water;
DOI:10.1021/jm00101a017