2-amino-5-chloro-3-benzyloxypyrazine

Base Information

Chemical Name:2-amino-5-chloro-3-benzyloxypyrazine
CAS No.:1410164-77-0
Molecular Formula:C₁₁H₁₀ClN₃O
Molecular Weight:235.673
Hs Code.:

Synonyms:2-amino-5-chloro-3-benzyloxypyrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-amino-5-chloro-3-benzyloxypyrazine

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Technology Process of 2-amino-5-chloro-3-benzyloxypyrazine

There total 1 articles about 2-amino-5-chloro-3-benzyloxypyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 873-42-7
3,5-dichloro-pyrazin-2-ylamine

: 1410164-77-0
2-amino-5-chloro-3-benzyloxypyrazine

Guidance literature:: benzyl alcohol; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.166667h; Inert atmosphere;

3,5-dichloro-pyrazin-2-ylamine; In tetrahydrofuran; mineral oil; for 24h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.09.039 DOI:10.1016/j.tet.2012.09.039

Reference yield: 50.0%

: 1410164-77-0
2-amino-5-chloro-3-benzyloxypyrazine

: 1410164-82-7
5-chloro-2-iodo-3-benzyloxypyrazine

Guidance literature:: 2-amino-5-chloro-3-benzyloxypyrazine; With hydrogen iodide; In water; acetonitrile; at 0 ℃; for 0.166667h; Inert atmosphere;

With sodium nitrite; In water; acetonitrile; at 0 - 50 ℃; for 21.1667h; Inert atmosphere;
DOI:10.1016/j.tet.2012.09.039 DOI:10.1016/j.tet.2012.09.039

Reference yield: 48.0%

: 1410164-77-0
2-amino-5-chloro-3-benzyloxypyrazine

: 1410164-87-2
5-chloro-2-bromo-3-benzyloxypyrazine

Guidance literature:: With copper(I) bromide; copper(ll) bromide; isopentyl nitrite; In acetonitrile; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2012.09.039 DOI:10.1016/j.tet.2012.09.039