C₆₂H₇₇NO₈

Base Information

Chemical Name:C₆₂H₇₇NO₈
CAS No.:1256563-97-9
Molecular Formula:C₆₂H₇₇NO₈
Molecular Weight:964.295
Hs Code.:

C<sub>62</sub>H<sub>77</sub>NO<sub>8</sub>

Synonyms:C₆₂H₇₇NO₈

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Chemical Property of C₆₂H₇₇NO₈

Chemical Property:

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Technology Process of C₆₂H₇₇NO₈

There total 11 articles about C₆₂H₇₇NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1256563-96-8
C₅₄H₇₂O₆

: 100-19-6
(4-nitrophenyl)ethanone

: 1256563-97-9
C₆₂H₇₇NO₈

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 24h; Reflux;
DOI:10.1021/ol102398y

Reference yield:

: 1256563-86-6
2,5-bishexyloxy-4-iodostyrene

: 1256563-97-9
C₆₂H₇₇NO₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / diethyl ether; hexane / 0 °C / Inert atmosphere

1.2: 2 h / 20 °C / Inert atmosphere

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform / 40 h / Inert atmosphere; Reflux

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / toluene / 20 h / 80 °C / Inert atmosphere

4.1: toluene-4-sulfonic acid / benzene / 24 h / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tetrabutylammomium bromide; potassium carbonate; toluene-4-sulfonic acid; In diethyl ether; hexane; chloroform; toluene; benzene; 3.1: Suzuki coupling / 4.1: Aldol condensation;
DOI:10.1021/ol102398y

Reference yield:

: 111-25-1
1-bromo-hexane

: 1256563-97-9
C₆₂H₇₇NO₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydrosulfite pentahydrate; tetrabutylammomium bromide; potassium hydroxide / water; toluene / Cooling with ice; Reflux

2.1: Iodine monochloride / methanol / Cooling with ice; Reflux

3.1: n-butyllithium / diethyl ether; hexane / 0.75 h / 0 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: n-butyllithium / diethyl ether; hexane / 0 °C / Inert atmosphere

5.2: 2 h / 20 °C / Inert atmosphere

6.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform / 40 h / Inert atmosphere; Reflux

7.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetrabutylammomium bromide; potassium carbonate / toluene / 20 h / 80 °C / Inert atmosphere

8.1: toluene-4-sulfonic acid / benzene / 24 h / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; sodium hydrosulfite pentahydrate; potassium tert-butylate; tetrabutylammomium bromide; Iodine monochloride; potassium carbonate; toluene-4-sulfonic acid; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; water; toluene; benzene; 4.1: Wittig reaction / 7.1: Suzuki coupling / 8.1: Aldol condensation;
DOI:10.1021/ol102398y