2,5-bishexyloxy-4-iodostyrene

Base Information

Chemical Name:2,5-bishexyloxy-4-iodostyrene
CAS No.:1256563-86-6
Molecular Formula:C₂₀H₃₁IO₂
Molecular Weight:430.369
Hs Code.:

Synonyms:2,5-bishexyloxy-4-iodostyrene

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Chemical Property of 2,5-bishexyloxy-4-iodostyrene

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Technology Process of 2,5-bishexyloxy-4-iodostyrene

There total 5 articles about 2,5-bishexyloxy-4-iodostyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1779-49-3
Methyltriphenylphosphonium bromide

: 2,5-bis(hexyloxy)-4-iodobenzaldehyde

: 1256563-86-6
2,5-bishexyloxy-4-iodostyrene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol102398y

Reference yield:

: 111-25-1
1-bromo-hexane

: 1256563-86-6
2,5-bishexyloxy-4-iodostyrene

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydrosulfite pentahydrate; tetrabutylammomium bromide; potassium hydroxide / water; toluene / Cooling with ice; Reflux

2.1: Iodine monochloride / methanol / Cooling with ice; Reflux

3.1: n-butyllithium / diethyl ether; hexane / 0.75 h / 0 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With n-butyllithium; sodium hydrosulfite pentahydrate; potassium tert-butylate; tetrabutylammomium bromide; Iodine monochloride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; water; toluene; 4.1: Wittig reaction;
DOI:10.1021/ol102398y

Reference yield:

: 67399-93-3
1,4-dihexyloxybenzene

: 1256563-86-6
2,5-bishexyloxy-4-iodostyrene

Guidance literature:: Multi-step reaction with 3 steps

1.1: Iodine monochloride / methanol / Cooling with ice; Reflux

2.1: n-butyllithium / diethyl ether; hexane / 0.75 h / 0 °C / Inert atmosphere

2.2: 2 h / 20 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With n-butyllithium; potassium tert-butylate; Iodine monochloride; In tetrahydrofuran; methanol; diethyl ether; hexane; 3.1: Wittig reaction;
DOI:10.1021/ol102398y