Technology Process of C21H27NO5S
There total 8 articles about C21H27NO5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C22H29NO5S;
With
lithium hydroxide;
In
tetrahydrofuran; methanol;
for 2h;
With
hydrogenchloride;
In
water;
- Guidance literature:
-
Multi-step reaction with 8 steps
1: sodium sulfite / water / 3 h / 0 - 20 °C
2: sodium hydroxide / water; methanol / 72 h / 20 °C
3: sulfuric acid; nitric acid / 1 h / 0 - 110 °C
4: sodium hydrogencarbonate / water / 85 °C
5: thionyl chloride / 60 °C
6: ammonium chloride; iron / water; ethanol / 2.25 h / 85 °C
7: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
8: lithium hydroxide / methanol; tetrahydrofuran / 2 h
With
thionyl chloride; sulfuric acid; nitric acid; sodium tris(acetoxy)borohydride; iron; sodium hydrogencarbonate; ammonium chloride; sodium hydroxide; lithium hydroxide; sodium sulfite;
In
tetrahydrofuran; methanol; ethanol; water; 1,2-dichloro-ethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: sulfuric acid; nitric acid / 1 h / 0 - 110 °C
2: sodium hydrogencarbonate / water / 85 °C
3: thionyl chloride / 60 °C
4: ammonium chloride; iron / water; ethanol / 2.25 h / 85 °C
5: sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C
6: lithium hydroxide / methanol; tetrahydrofuran / 2 h
With
thionyl chloride; sulfuric acid; nitric acid; sodium tris(acetoxy)borohydride; iron; sodium hydrogencarbonate; ammonium chloride; lithium hydroxide;
In
tetrahydrofuran; methanol; ethanol; water; 1,2-dichloro-ethane;
