Technology Process of C35H33ClGeN2O2
There total 3 articles about C35H33ClGeN2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C35H36N2O2;
With
sodium hydride;
In
tetrahydrofuran;
at 20 ℃;
for 1.5h;
Glovebox;
Inert atmosphere;
germaniumtetrachloride;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 15h;
Glovebox;
Inert atmosphere;
DOI:10.1021/ja5046814
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane / 4.5 h / 20 °C / Schlenk technique; Inert atmosphere; Darkness
1.2: 2 h / 20 °C / Schlenk technique; Inert atmosphere
2.1: sodium dodecanethiolate / N,N-dimethyl-formamide / 40 h / 20 - 110 °C / Schlenk technique; Inert atmosphere
3.1: sodium hydride / tetrahydrofuran / 1.5 h / 20 °C / Glovebox; Inert atmosphere
3.2: 15 h / 0 - 20 °C / Glovebox; Inert atmosphere
With
sodium dodecanethiolate; sodium hydride; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja5046814
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid / dichloromethane / 4.5 h / 20 °C / Schlenk technique; Inert atmosphere; Darkness
1.2: 2 h / 20 °C / Schlenk technique; Inert atmosphere
2.1: sodium dodecanethiolate / N,N-dimethyl-formamide / 40 h / 20 - 110 °C / Schlenk technique; Inert atmosphere
3.1: sodium hydride / tetrahydrofuran / 1.5 h / 20 °C / Glovebox; Inert atmosphere
3.2: 15 h / 0 - 20 °C / Glovebox; Inert atmosphere
With
sodium dodecanethiolate; sodium hydride; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja5046814
