C₃₆H₆₀O₆Si

Base Information

Chemical Name:C₃₆H₆₀O₆Si
CAS No.:1109115-17-4
Molecular Formula:C₃₆H₆₀O₆Si
Molecular Weight:616.954
Hs Code.:

C<sub>36</sub>H<sub>60</sub>O<sub>6</sub>Si

Synonyms:C₃₆H₆₀O₆Si

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Chemical Property of C₃₆H₆₀O₆Si

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Technology Process of C₃₆H₆₀O₆Si

There total 11 articles about C₃₆H₆₀O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1109114-93-3
C₃₆H₅₈O₆Si

: 1109115-17-4
C₃₆H₆₀O₆Si

Guidance literature:: With acetic acid; tetramethylammonium triacetoxyborohydride; In acetonitrile; at -30 - 20 ℃; for 36h; diastereoselective reaction;
DOI:10.1039/c5ob00498e

Reference yield:

: C₂₆H₄₁BO₃

: 1109115-17-4
C₃₆H₆₀O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1: lithium borohydride / tetrahydrofuran / 19.5 h / -78 - -20 °C

2: sodium hydroxide; dihydrogen peroxide / water; methanol / 3 h / 20 °C

3: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / -10 °C / Molecular sieve

4: 1H-imidazole / dichloromethane; benzene / 0.5 h / 20 °C

5: diisobutylaluminium hydride / dichloromethane / 2 h / -78 - 0 °C

6: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

7: diethyl ether / 17.5 h / -78 - -23 °C

8: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 36 h / -30 - 20 °C

With 1H-imidazole; lithium borohydride; dihydrogen peroxide; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetonitrile; benzene;
DOI:10.1039/c5ob00498e

Reference yield:

: 182193-69-7
(S)-1-(p-methoxybenzyloxy)-2-methylpentan-3-one

: 1109115-17-4
C₃₆H₆₀O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1: triethylamine / diethyl ether / 1.5 h / 0 °C

2: lithium borohydride / tetrahydrofuran / 19.5 h / -78 - -20 °C

3: sodium hydroxide; dihydrogen peroxide / water; methanol / 3 h / 20 °C

4: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / -10 °C / Molecular sieve

5: 1H-imidazole / dichloromethane; benzene / 0.5 h / 20 °C

6: diisobutylaluminium hydride / dichloromethane / 2 h / -78 - 0 °C

7: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.5 h / 20 °C

8: diethyl ether / 17.5 h / -78 - -23 °C

9: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 36 h / -30 - 20 °C

With 1H-imidazole; lithium borohydride; dihydrogen peroxide; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetonitrile; benzene;
DOI:10.1039/c5ob00498e